Covalent

Nanoprobing

From Imaging to Electrical Insight—All in One Workflow Covalent offers in-situ nanoprobing for targeted electrical characterization and failure analysis on nanoscale features inside our JEOL PS500i FIB-SEM.

What is Nanoprobing? 

Nanoprobing is an in-situ technique that uses ultra-fine probe tips to make direct electrical contact with microscopic features inside an electron microscope. By positioning probes onto specific device structures under high magnification, engineers can measure local electrical behavior—such as current–voltage (I–V) response—at the region of interest.

Unlike traditional optical probe stations, nanoprobing is performed inside an SEM or dual-beam system, allowing you to see with higher precision where the probes are landing and the landing force. This enables direct correlation between a device’s physical structure and its electrical performance while preserving the features, which is critical for advanced semiconductor failure analysis and device debugging.

In practice, nanoprobing turns the microscope from a purely imaging, spectroscopy, and crystal structure tool into a functional test platform—letting you not only find a feature or defect, but also determine how it behaves electrically in real time.

Compatible with SEM and Dual Beam Workflows

Use nanoprobing alongside high-resolution imaging, tilt-based workflows, and site-specific failure analysis methods.

Localized Electrical Behavior

Measure electrical behavior where you see the feature, defect, or structure of interest inside the microscope.

Flexible, Modular Platform

Adapt the system for different samples, chambers, and applications with configurable probe count, accessories, and software-guided workflows.

Why use Nanoprobing? 

Nanoprobing adds direct electrical interaction to the same SEM workflow already used for imaging, navigation, and site-specific analysis. Instead of stopping at visual/elemental/crystallographic inspection, you can land probes on structures of interest and measure how a device behaves electrically at the nanoscale.

See, Contact, Measure

Visually navigate to a feature, land probes with precision, and immediately measure electrical response at that location.

Fast Approach, Precise Landing

Move quickly across the sample with coarse positioning, then switch to nanometer-scale control for accurate and repeatable probe contact.

Stable Measurements Over Time

Maintain reliable electrical contact on small structures for extended measurements, even under tilt and high-resolution imaging conditions.

How Nanoprobing Works

Nanoprobing operates by bringing ultra-fine conductive probe tips into direct contact with specific features on a sample inside an electron microscope. Using high-resolution SEM or dual-beam imaging for navigation, the user first locates the region of interest—such as a transistor gate, interconnect, or suspected defect site—then positions the probes with nanometer-scale precision using multi-axis manipulators. Coarse motion enables rapid positioning across the sample, while fine motion allows controlled, gentle landing of the probe tips onto targeted structures without damaging them.

Close-up of advanced electronic hardware and wiring for blockchain tech.

Once contact is established, electrical measurements such as current–voltage (I–V) response, resistance, or continuity can be performed in situ. Because the process occurs inside the microscope, the probe location is visually confirmed, enabling direct correlation between physical structure and electrical behavior. This integration is what distinguishes nanoprobing from traditional probe stations: instead of testing blindly at predefined pads, users can interrogate specific nanoscale features, defects, or interfaces in real time, and immediately connect what they see to how the device performs

Equipment Used for Nanoprobing

We use the Talos™ F200X G2 TEM with Super-X EDS system for DPC and other Transmission Electron Microscopy needs. 

Imina NANO

Platform type: integrated into our JEOL FIB SEM.
Core motion concept: Compact mobile nanoprobers with independent multi-axis control
Degrees of freedom: 4 degrees of freedom per nanoprober
Probe count: 4
Positioning resolution: Nanometer-scale fine positioning
Coarse motion range: Up to centimeter-scale travel for rapid approach to the region of interest
Fine motion range: Up to ~15 µm at the probe tip for precise contact landing
Working conditions: Compatible with short working distances, low accelerating voltage imaging, and high-resolution magnetic-lens imaging conditions
Tilt compatibility: Supports tilt-compatible workflows, with stable contact maintained at angles used for FIB operations
Probe tips: Industry-standard tungsten probe tips, with very fine tip-radius options
Software: Integrated control software for probe positioning, measurement setup, workflow guidance, data handling, and reporting

Specifications

Key Differentiators

TXRF is a technique distinguished by its exceptional surface sensitivity, ultra-trace detection limits, and non-destructive measurement, but it also has key technical constraints.

Strengths

  • Direct electrical testing at the site of interest
  • Real-time correlation between structure and electrical behavior
  • Nanometer-scale probe placement for localized measurements
  • Compatible with SEM and dual-beam workflows
  • Useful for films, particles, transistors, interconnects, defects, and failure-analysis studies
  • Stable contact for extended in-situ electrical measurements
  • Flexible platform for a wide range of microelectronic and research devices

Limitations

  • Stable contact can be difficult on very small, oxidized, contaminated, or highly topographic features
  • Better suited for targeted analysis than high-throughput production testing
  • Requires exposed or accessible structures for reliable probe landing
  • Measurement quality depends heavily on sample condition, geometry, and operator setup
  • Often most effective when combined with correlative imaging or cross-sectioning workflows

Example Outputs

Probing at exposed alumina parts to investigate low ohmic VIA chains.
Resistivity measurement of VIA chains.
Electrical probing of a single PMOS transistor.
Transistor characteristics: I/V curves function of different gate voltage potentials.

Sample Requirements

Measurement success depends on surface and sample preparation. We can help with sample preparation.

  • Solid phase.
  • Must be vacuum stable.
  • Maximum Sample Height: 55 mm.
  • Maximum Sample Weight: 500 g (including sample-holder).
  • Maximum Lateral Dimension: 150 mm (larger samples enabled with reduced rotation).

Nanoprobing Applications by Industry

Semiconductor Failure Analysis

Nanoprobing is used to electrically interrogate localized areas of a failing device, helping connect electrical behavior to the physical site under investigation.

Device Characterization and Debug

Supports in-situ I–V measurements on microelectronic structures to evaluate local device behavior and compare suspect vs. nominal regions.

FIB Delayering to Probe Buried Structures

Delayer the sample and probe exposed surfaces in one tool.

Research Materials and Micro/Nanodevices

Nanoprobing can also be used for localized testing of MEMS, sensors, nanowires, thin films, nanoparticles, graphene, microLEDs, solar cells, and other research-scale devices where direct electrical access under the microscope is valuable.

Correlative Probing with FIB or SEM Review

Combine imaging, probing, and follow-on analysis such as FIB cross-sectioning for deeper root-cause investigation.

Thin Film 4 Point Probe

Investigate sheet resistance in thin films.

Techniques That Complement Nanoindentation

Site-specific cross-sectioning and structural analysis
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Atomic-scale structural characterization after localization.
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EDS
Elemental analysis at the probed location.
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Atomic Force Microscopy (AFM) Analysis

AFM scans a sharp probe to map nanoscale topography and material properties with sub‑nanometer sensitivity.

Nanoscale surface and topography analysis.
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SIMS or XPS

XPS measures surface elemental composition and chemical states within ~7–10 nm, enabling angle-resolved and depth profiling.

Nanoscale surface and topography analysis.
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Frequently Asked Questions

What is nanoprobing used for?

Nanoprobing is used to contact small device features and measure local electrical behavior directly inside a microscope.

What makes nanoprobing different from a traditional probe station?

Nanoprobing allows you to see and contact features at high magnification inside the SEM or FIB, enabling precise correlation between structure and electrical behavior.

Can nanoprobing be used with FIB workflows?

Yes. Nanoprobing systems are compatible with tilted geometries used in FIB workflows, enabling correlative analysis and in-situ workflows at the same site of interest.

What kinds of samples can be tested?

Semiconductor devices, interconnects, MEMS, nanowires, thin films, sensors, optoelectronic devices, and other solid-state structures that can be accessed in the microscope.